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Application areas and drugs of Egyptian, Greek and Roman medi-cine are popular references of research in the field of recent aes-thetic dermatology. There, Cleopatra VII is referred to as “mother of chemical peeling” because she is said to have bathed in donkey’s milk. Although extremely popular, there is no ancient source sup-porting Cleopatra’s bath in milk. Nevertheless, Poppaea Sabina, the second wife of Emperor Nero, is said to has bathed in donkey’s milk to beautify her skin. The aim of the paper is to reconstruct the genesis and develop-ment of the modern myth of Cleopatra bathing in donkey’s milk. The origin of this myth can be traced back to the cinema of the 1930s. The result is that in the person of the actress Claudette Colbert her two roles as Cleopatra and Poppaea converged. This convergence was the basis for the popularization of the milk bath by the Cleopat-ra movie of 1963 with Elizabeth Taylor.
Nicht nur der Lauf der Geschichte verändert sich, sondern auch Geschichtswissenschaft und -unterricht. An die Stelle des Auswendiglernens vorgegebener historischer Erzählungen trat im Laufe der Zeit zunehmend die Befähigung zu deren Dekonstruktion. Dafür müssen allerdings die Entstehungsbedingungen (geschichts-)wissenschaftlicher Erkenntnisse nachvollzogen werden können. Eine Möglichkeit, dies auf spielerische Art und Weise, aber auch auf Augenhöhe mit Lehrkräften und Historiker*innen zu tun, bieten Open-World- Spiele wie HORIZON ZERO DAWN (2017).
„Gut, besser, Vermesser.“
(2021)
Die Geschichte der Mikrobiologie als Laborwissenschaft des späten 19. Jahrhunderts hat für Ehrenberg keinen Platz. Unmodern, ja fehlerhaft scheinen die Befunde dieses „Humboldt en miniature“, der die Belebtheit von Wasser oder Luft mikroskopisch untersuchte, der Proben aus aller Welt sammelte und so zahlreiche „Infusorien“ genannte Mikroben sowie deren Effekte etwa bei Blutwundern beschrieb, deren Beteiligung an Infektionskrankheiten aber verneinte. Zugleich scheint sein ökologischer Blick auf den Mikrokosmos die Gegenwart auf überraschende Weise anzusprechen – einerseits weil Mikroben omnipräsentes Faszinosum wie Bedrohung bleiben, andererseits weil viele der Prämissen von Pasteur und Koch im Zeitalter der Genomik überholt erscheinen. Ausgehend von der zwiespältigen Position Ehrenbergs fragt dieser Artikel, warum er möglicherweise gerade deswegen spannender ist, als ihn die Historiographie bislang hat erscheinen lassen.
A quote from Fight Club (Chuck Palahniuk, 1996) may seem unusual for a Classicist. Nevertheless, this famous sentence summarises the contents of this special issue of thersites perfectly. As specialists in classical reception frequently witness, there is a sort of déjà-vu effect when it comes to the presence of Antiquity within popular culture. In 2019, to try to better understand the phenomenon, Antiquipop invited researchers to take an interest in the construction and semantic path of these “masterpieces” in contemporary popular culture, with a particular focus on the 21st century.
“Chunking” spoken language
(2021)
In this introductory paper to the special issue on “Weak cesuras in talk-in-interaction”, we aim to guide the reader into current work on the “chunking” of naturally occurring talk. It is conducted in the methodological frameworks of Conversation Analysis and Interactional Linguistics – two approaches that consider the interactional aspect of humans talking with each other to be a crucial starting point for its analysis. In doing so, we will (1) lay out the background of this special issue (what is problematic about “chunking” talk-in-interaction, the characteristics of the methodological approach chosen by the contributors, the cesura model), (2) highlight what can be gained from such a revised understanding of “chunking” in talk-in-interaction by referring to previous work with this model as well as the findings of the contributions to this special issue, and (3) indicate further directions such work could take starting from papers in this special issue. We hope to induce a fruitful exchange on the phenomena discussed, across methodological divides.
“Chunking” spoken language
(2021)
In this introductory paper to the special issue on “Weak cesuras in talk-in-interaction”, we aim to guide the reader into current work on the “chunking” of naturally occurring talk. It is conducted in the methodological frameworks of Conversation Analysis and Interactional Linguistics – two approaches that consider the interactional aspect of humans talking with each other to be a crucial starting point for its analysis. In doing so, we will (1) lay out the background of this special issue (what is problematic about “chunking” talk-in-interaction, the characteristics of the methodological approach chosen by the contributors, the cesura model), (2) highlight what can be gained from such a revised understanding of “chunking” in talk-in-interaction by referring to previous work with this model as well as the findings of the contributions to this special issue, and (3) indicate further directions such work could take starting from papers in this special issue. We hope to induce a fruitful exchange on the phenomena discussed, across methodological divides.
Die aktuelle Politik der Europäischen Union hat im Umgang mit flüchtenden Menschen das Mittelmeer in ein Massengrab verwandelt. Dass auch im Jahr 2021 täglich Menschen an den EU-Außengrenzen sterben hängt dabei mit dem Ausbau von Sicherheitsmechanismen zum Zweck eines verstärkten Grenzschutzes zusammen. Durch Sicherheitsmechanismen wie bspw. den Ausbau von Frontex und die elektronische Erfassung von Ein- und Ausreisedaten schottet sich die EU dabei immer weiter ab während gleichzeitig die Thematik der Flucht und Migration eine zunehmende ‚Versicherheitlichung‘ erfährt.
Die vorliegende Arbeit geht davon aus, dass die Grundzüge der Versicherheitlichung von Flucht und Migration bereits im liberalen Staatsverständnis der EU angelegt sind. Mithilfe einer foucaultschen Diskursanalyse hinterfragt die Arbeit daher die historisch entstandenen und im Liberalismus inbegriffenen Vorannahmen über nicht-europäische Menschen und deren Fortentwicklung in die heutigen Politiken der EU. Dabei geht die Arbeit einerseits der Frage nach, wie sich die zunehmende Versicherheitlichung der Migration und der damit verbundene Umgang mit Nicht-Europäer*innen an den EU-Außengrenzen erklären lässt. Vertieft wird gefragt, inwieweit sich die konstruierten Wissensmuster über das europäische ‚wir‘ und die nicht-europäischen ‚Anderen‘ aus dem Liberalismus in der heutigen EU-Politik wiederfinden.
Auf Basis der Werke Michel Foucaults führt die Arbeit in die Entwicklung liberaler Staatlichkeit seit dem 17. Jahrhundert ein. Ergänzt werden diese Darstellungen um eine postkoloniale Perspektive, die eine Darstellung des liberalen Denkens über das europäische ‚Außen‘ vermittelt. Gemeinsam legen diese beiden Perspektiven die Strukturen liberalen Denkens offen, die im späteren Verlauf der Analyse in aktuellen EU-Dokumenten wiedererkannt werden. Als Analysedokumente dienen dabei sechs von der EU veröffentlichte Agenden, Verordnungen und Strategien, die die thematische Schnittstelle zwischen Sicherheit und Migration umfassen.
Die Ergebnisse zeigen, dass sich ein ‚Othering‘ - die historisch entstandene Gruppenbildung des homogen begriffenen europäischen ‚Wirs‘ gegenüber den nicht-europäischen ‚Anderen‘ - in der heutigen Politik der EU an deren Außengrenzen reproduziert. Das im 17. Jahrhundert entstandene Sicherheitsdenken des liberalen Staates wird über die Reproduktion bestimmter Wissensmuster in Form von ‚Stories‘ auf die heutigen EU-Außengrenzen übertragen. Nach ‚innen‘ handelt die EU dabei nach einem Grundsatz der ‚gemeinsamen Stärke‘ der europäischen Staaten bzw. der EU-Mitgliedstaaten, während nach ‚außen‘ eine zweckrationale Kooperation mit Drittstaaten verfolgt wird. Statt um die Wahrung von Menschenleben geht es damals wie heute v.a. um den Vorteil Europas bzw. der EU. Von diesen Ergebnissen ausgehend wird die Zunahme der Versicherheitlichung von Flucht und Migration an den EU-Außengrenzen durch die Reproduktion des geschichtlich entstandenen Sicherheitsdenkens erklärt.
‘Smart’ Janus emulsions
(2021)
Emulsions constitute one of the most prominent and continuously evolving research areas in Colloid Chemistry, which involves the preparation of mixtures or dispersions of immiscible components in a continuous medium. Besides conventional oil-in-water or water-in-oil emulsions, other emulsions of complex droplet morphologies have recently attracted significant research interests. Especially Janus emulsions, in which each droplet is comprised of two distinct sub-regions, have shown versatile potential applications. One of their advantages is the possibility of compartmentalization, which enables to play with two different chemistries in a single droplet. Though microfluidic methods are conventionally used to prepare Janus emulsions, their industrial applications are largely hindered by low throughput and extensive instrumentations. Recently, it has been discovered that simply one-pot moderate/high energy emulsification is also capable of developing Janus morphology, although their preparation and stabilization remain rather substantially challenging. This cumulative doctoral thesis focuses on the preparation and characterization of ‘smart’ Janus emulsions, i.e. Janus emulsions with special stimuli-responsive features. One-step moderate/high energy emulsification of olive and silicone oil in an aqueous medium was carried out. Special consideration was devoted to the interfacial tensions among the components to maintain the criteria of forming characteristic droplet architectures, in addition to avoiding multiple emulsion destabilization phenomena like imminent phase separation or even separated droplet formation. A series of investigations were conducted related to the formation of complexes of charged macromolecules and role of them as stabilizers to achieve stable Janus emulsions for a realistic timeframe (more than 3 months). The correlation between the size of the stabilizer particles and the droplet size of emulsion was established. Furthermore, it was observed that Janus emulsion gels with interesting rheological properties can be fabricated in the presence of suitable polyelectrolyte complexes. Janus emulsions that could be influenced by pH, temperature or magnetic field were successfully produced in presence of characteristic stimuli-responsive stabilizers. Afterwards, the effect of these changes was studied by different characterization techniques. The size and morphology could be tuned easily by changing the pH. The incorporation of iron oxide magnetic nanoparticles (synthesized separately by a co-precipitation method) to one component of the Janus emulsion was carried out so that the movement and orientation of the complex droplets in aqueous media could be controlled by an external magnetic field. Additionally, temperature-triggered instantaneous reversible breakdown of Janus droplets was also accomplished. The responses of the Janus droplets by the stimuli were well-documented and explained. Another goal of the present contribution was to exploit this special morphological feature of emulsions as a template for producing porous materials. This was demonstrated by the preparation of ultralight magnetic responsive aerogels, utilizing Janus emulsion gels. The produced aerogels also showed the capacity to separate toxic dye from water. To the best of our knowledge, this is the first example of investigation towards batch scale production of Janus emulsion with such special stimuli-responsive properties by a simple bulk emulsification method.
‘La poesía no da para tanto’
(2021)
Este artículo se enfoca en la singular combinación de poesía, ficción y autobiografía que pone en juego la obra reciente de Lorenzo García Vega. A través de una lectura de dicha obra, y en particular de la ‘mala novela’, Devastación del Hotel San Luis (2007), se propone un replanteamiento teórico del concepto de autoficción que se apoya en el análisis lingüístico de los modos de enunciación de Benveniste y en una revisión de la teoría de los géneros literarios de Käte Hamburger. Mi lectura sitúa la cuestión de la autoficción en el conflictivo diálogo de este autor con el grupo Orígenes, y explora el cruce de modos narrativos y líricos de autofiguración en el singular proyecto de García Vega: reescribir la narrativa autobiográfica proustiana a la vez que la poética neobarroca lezamiana.
העבודה הזאת עוסקת בנצרות הקדומה ובשלבי התפתחותה במאה הראשונה לספירה. הדגש בעבודה הוא על יחסי הגומלין בין הנצרות ל ארץ הקודש. המחקר הזה מציע קריאה אלטרנטיבית של המקורות העבריים הקדומים, שלפיה התנועה של ישו ההיסטורי נתפסת כתוצר של השיח הת יאולוגי והפוליטי באו תה תקופה בגליל וביהודה. הקריאה המוצעת מאתגרת את המגמה המקובלת בספרות המחקר, אשר נוטה להפריד לא רק בין ישו לבין הקשרו הדתי, אלא גם בין אלמנטים דתיים לפוליטיים בנצרות הקדומה. מטרת מחקר זה היא לאפשר הסתכלות מקומית על הנצרות של המאה הראשונה כחלק בלתי נפרד מן התמונה הפלסטינית הדתית והפוליטית הרחבה.
המחקר מחולק לחמשה פרקים. הפרק הראשון מציג רקע היסטורי לכיתות וזרמי היהדות בארץ הקודש במאה הראשונה מנקודת מבט דתית -פוליטית. הפרק הזה מעמיק את ההבנה של גווני התודעה ההיסטורית של אנשי ארץ הקודש במאה הראשונה לספירה. הפרק השני מציג את תולדות הנצרות של ישו ההיסטורי בשיטה תימטית , שמאירה את התהליך המורכב שישו והעם הפלסטיני-יהודי עבר בתקופה הזאת. שלושת הת ימות בפרק השני הן: ההלכה של ישו )כשרות ושבת(; המרד השקט )המשמעות הפוליטית של פסטיבל הפסח בירושלים עבור יהודי הבית השנ י(; והגאולה עלי אדמות על פי ישו המתואר בספרי הבשורה. הפרק השלישי מציג את תולדות הנצרות על פי פאולוס. הפרק מתמקד בהעברת ישו מירושלים לרומא, ודן בתוצאות המעבר הזה תוך הדגשת השלכותיו על הדור הנוצרי הראשון ועל ארץ הקודש.
הפרק הרביעי הוא פרק "הנצרות הפלסטינית" שמסכם את שלושת הפרקים הקודמים, ומציע קריאה פוסט- קולוניאלית של הנצרות הפלסטינית של ישו ההיסטורי )היהודי( אל מול הנצרות הרומית שהתבססה מאוחר יותר על הת יאולוגיה של פאולוס. הפרק הזה מסביר מדוע חשוב לחבר מחדש בין הדתי לפוליטי, ומדגיש כי ההשקפה האוניברסאלית הידועה של הנצרות לא הייתה חלק מתנועתו של ישו, מכיוון שישו ההיסטורי היה מונע על ידי היותו יהודי, עם תחושת שייכות גבוהה לקהילתו הפלסטינית -יהודית, ולא על ידי כך שהוא הבן של אלוהים. הפרק החמישי הוא פרק הסיום, ובו מוצג סיכום קצר, ויש בו סקירה של השלכות תיאורטיות של עבודת מחקר זו והמלצות למחקרים עתידיים.
"מגילת שיר השירים היא יצירה עתיקה וחידתית. מילותיה הייחודיות שזורות ביד אמן. תשומת לב למלאכת רקמה עדינה זו ולהתכתבותה עם מקורות מקראיים אחרים פותחת נתיבי פרשנות מפתיעים. הספר 'מי זאת עולה מן המדבר' מציע שלוש קריאות במגילה ועונה לשאלה 'מי זאת' שלוש תשובות מהפכניות:• הקריאה הראשונה עוסקת ביחסים שבין גברים ונשים ובקשר שבין אהבה וחופש. הקול הנשי העולה בה הוא קולה של אישה המתבוננת בדפוסי הזוגיות המוכרים לה וקוראת לשינוי מהותי בהם.• הקריאה השנייה עוסקת ביחסים שבין האדם והאלוהות. הדמות הנשית המתגלה בו היא דמותה של האלוהות החושפת את מנגנוני הכוח שבממסד הדתי ומציעה לאדם קשר המושתת על חירות ואהבה.• בקריאה השלישית הדמות הנשית היא ההוויה כולה. היא עוסקת בקשר שבין ההוויה לתודעה האנושית החופשית במהותה ובאפשרות של השפה לחבר ביניהן באהבה.יחד, הקולות הנשיים הללו מציעים לנו, כחברה וכיחידים, תהליך צמיחה שבליבו אהבה וחירות החיוניות זו לקיומה של זו."שיר השירים הוא שירת הפצעה גדולה של אהבה. כוח אהבה, שאין דבר שישווה לו מבין כל כוחות עולם. אבל ההפצעה הזו, מקורה בפצע, פצע שכולנו נושאות ונושאים בתוכנו כבר דורי דורות, פצע הקשר בין גברים ונשים. כמה לא מתואמות יכולות להיות השפות שלנו על הציר המתעתע שבין תאווה לאהבה, כמה אי הלימה יכולה להיות בין שפת האם של השכינה והאשה, שפת אתיקה של אהבה, של נאמנות, לשפות אהבה שהן במסווה ובנתק. ואיך נצמיח בעולם אהבת אמת, עדינה, חופשייה ושלמה.פירושה של מרב מזא"ה הוא רגע היסטורי. בדור פצוע אהבה, בשפה ברורה ובהירה, שכבה אחר שכבה, בסבלנות ובחכמה של התגלות, לוקחת מרב את קוראיה למסע אל עומק הפצע. בהלימה בין תוכן המגילה לצורה בה בחרה לכתוב את פירושה, בבחירה ללכת עם הקוראים לאט את המסע כולו, פסוק אחר פסוק, במסע שכוחו לא רק בפענוח אלא גם בקצב המוענק לכל קורא על פי דרכו, נותנת מרב הזדמנות לכל אחת ואחד לצלול אל המגילה, לכאוב איתה ולהירפא מכוחה. מסע שיר השירים הוא הזמנה עתיקה ונמשכת שהגיעה שעתה, הזמנה לנשים וגברים לכאוב יחד את נתק הקשר, לשמוע זה את קולו של זו, לספר את פציעות הלב והגוף, ולהתגלות זו לזה במסע אמון ואמונה, איחוי וריפוי, מסע אהבת אמת העולה לרגל לירושלים, אל השלם." -- מן המעטפת האחורית.
לא מעט ביוגרפיות חשובות מרחיבות דעת ומשכילות נכתבו על אודות איש הרוח והפילוסוף מרטין בובר – הוגה עז רושם, שהדי הגותו, אמרותיו וכתביו אוחזים בנו גם היום למעלה מחצי מאה לאחר מותו. יחד עם זאת, כל הביוגרפיות יחדיו, חשובות ומעמיקות כפי שהן, אינן משתוות בעצמתן הספרותית לספרון קצר זה, שניתן לראות בו מעין אוטוביוגרפיה מזוקקת הכתובה בצורה של פרגמנטים קצרים.
לא בכדי השווה מוריס פרידמן את העצמה הפואטית-פילוסופית של הפרגמנטים האוטוביוגרפיים שלפנינו אל ספריו של בובר אני ואתה (1923) ודרכו של אדם על פי תורת החסידות (1948). אכן בזכרונות אלו שבובר מעלה טבוע משהו מן הטון של סיפורי החסידות ומן המסר של הפילוסופיה הדיאלוגית. ואולם, בניגוד לשני הספרים הקודמים שהוזכרו, פגישות לא נכתב כספר אלא הפך לספר בדיעבד. זוהי למעשה אסופה של זכרונות קצרים ומלאי תובנה שנכתבו ופורסמו בזמנים שונים וראו אור לראשונה כיחידה אחת באסופת המאמרים אודות הפילוסופיה של מרטין בובר (1967), בעריכתם של ארתור שליפ ומוריס פרידמן. מוריס פרידמן מעיד שהיה שותף לבחירה, סידור ולעריכה של הפרגמנטים שלפנינו יחד עם בובר, ובעוד שחלק מהפרגמנטים פורסמו בתקופות מוקדמות יותר, חלקם נכתבו לכבוד האסופה. פרידמן אף מדגיש את ערכם המעשי של סיפורי פגישות אלה בדינמיקות קבוצתיות ובסמינרים ואת כוחם לעורר בקורא זיכרונות וחוויית אישיים.
Настоящий научно-практический комментарий и перевод Уголовного уложения Федеративной Республики Германия не ограничивается собственно трансформацией текста основного уголовного закона Германии на русский язык. Руководствуясь принципами функционального перевода, автор посредством точного и систематического перевода доводит до сведения читателя смысл уголовно-правовых норм. Научно-практический комментарий к Уголовному уложению Германии представляет собой постатейный комментарий, учитывающий как мнение законодателя, так и мнение правоприменительной практики Федерального Верховного суда и высших Земельных судов Германии, а также немецкой юридической доктрины по основным проблемам уголовного права. Необходимое внимание было уделено также дополнительному уголовному праву и уголовно-процессуальным проблемам. Таким образом, задачей настоящего издания является предоставить читателю возможность правильного языкового понимания и юридического толкования уголовно-правовых норм Германии.
Вступительная статья «Введение в уголовное право Германии» содержит общий обзор немецкого уголовного права. Особое внимание уделено развитию и источникам уголовного законодательства, а также доктрине уголовного права ФРГ.
Книга может заинтересовать практиков и правоведов, а также всех, кто в своей профессиональной деятельности или в процессе обучения сталкивается с уголовным правом Германии.
Неблагоприятные последствия, наступившие в процессе осуществления медицинской деятельности, с правовой точки зрения оценивались неоднозначно во все времена. В отечественной истории были периоды, когда лекарей казнили даже без установления их вины и когда докторов вообще не привлекали к ответственности за допущенные ими нарушения. В настоящее время медицинская и фармацевтическая деятельность представляет собой сложный процесс выполнения профессиональных функций, связанный с соблюдением установленных стандартов и требований к его организации. Большинство медицинских обследований и манипуляций, имеющих профилактическую, исследовательскую, диагностическую, лечебную или реабилитационную направленность, регламентировано формальными рамками протокола, который может в одной ситуации не позволить компетентному врачу спасти жизнь пациента, а в другой - причинить вынужденный вред его здоровью. Обе обозначенные ситуации потребуют правовой оценки содеянного, механизм которой до сих пор в полной мере не определен. Данное обстоятельство может повлечь привлечение медицинского работника к уголовной ответственности при отсутствии (или неочевидности) вины в его действиях. С другой стороны, структурно сложная профессиональная деятельность, не имеющая признанных методик правовой оценки, создает предпосылки для различного рода нарушений и злоупотреблений со стороны медицинских работников. Меняющиеся отношения между врачом и пациентом, а также коммерциализация современной медицинской практики привели к тому, что система здравоохранения сегодня является одной из самых деликто- и даже криминально ориентированных. Изложенное выступает причиной усложняющегося законодательства (в широком смысле слова) об уголовной ответственности медицинских работников и противоречивой правоприменительной практики, а это, в свою очередь, порождает научные исследования данных проблем. Результаты таких исследований часто существуют вне связи с другими достижениями уголовно-правовой науки, поэтому представляется необходимым изучить развитие права, включая правоприменение и доктрину, об уголовной ответственности медицинских работников - медицинское уголовное право. С учетом того что для отечественной науки выделение такой подотрасли права является нетрадиционным, в настоящей работе представлены результаты исследования развития медицинского уголовного права не только в России, но и в Германии, где уже давно сложилась и обособилась данная область права.
Research has characterized Nadezhda Teffi as the female Chekhov.1 However, connections can also be found between her work and that of Ivan S. Turgenev. In particular the one-act plays (Conversation on a Highroad; 1851) and (The Woman Question; 1907) are suitable for comparison. Not only does my comparison consider the gender conflict between man and woman, but also a dialectic method which Teffi may have discovered in Turgenev's work and elaborated further. The dialectical considerations are connected with different comic approaches: the psychological comedy of the realist Turgenev in the middle of the 19th century and the mechanical comedy of the utopian Teffi at the start of the 20th century. Its mechanical comicality shows that relates to an international debate, in which Paul Julius Mobius' essay 'Uber den physiologischen Schwachsinn des Weibes' ('On the Physiological Idiocy of the Female'; 1900) may well have played an unfavourable role.
This paper attempts to account for the syntactic distribution of the particle sey in Turkish, in particular its suffixed variant which is a placeholder for expressions that have to be inserted into the discourse later. The paper argues that the distribution of suffixed sey is determined by constituent structure, meaning that Bey can only substitute for syntactic constituents. Thus, sey acts as a pro-form, similar, for instance, to pronouns substituting for noun phrases. This has two implications: First, as sey is a quasi-universal pro-form with the ability to substitute for a wide range of constituents, sey-substitution can be used as a constituency test to peek into the constituent structure of virtually any major syntactic domain. Second, the overall sey-substitution pattern across different syntactic domains constitutes evidence for Kayne's binary branching hypothesis.
Innerhalb dieser Arbeit erfolgte die erstmalige systematische Untersuchung von Vinylsulfonsäureethylester (1a), Phenylvinylsulfon (1b), N-Benzyl-N-methylethensulfonamid (1c) in der FUJIWARA-MORITANI Reaktion (alternativ als DHR bezeichnet). Bei dieser übergangsmetallkatalysierten Reaktion erfolgt der Aufbau einer neuen C-C-Bindung unter der doppelten Aktivierung einer C-H-Bindung. Somit kann ein atomökonomischer Aufbau von Molekülen realisiert werden, da keine Beiprodukte in Form von Salzen entstehen. Als aromatischer Reaktant wurden Acetanilide (2) verwendet, damit eine regiospezifische Kupplung durch die katalysatordirigierende Acetamid-Gruppe (CDG) erfolgt. Für die Pd-katalysierte DHR wurde eine umfangreiche Optimierung durchgeführt und anschließend konnten neun verschieden, substituierte 2 mit 1a und sieben verschieden, substituierte 2 mit 1b funktionalisiert werden. Da eine Reaktion mit 1c ausblieb, erfolgte ein Wechsel auf eine Ru-katalysierte Methode für die DHR. Mit dieser Methode konnte 1c mit Acetaniliden funktionalisiert werden und das Spektrum der verwendeten 2, in Form von deaktivierenden Substituenten erweitert werden.
Im Anschluss wurden die sulfalkenylierten Acetanilide in weiterführenden Reaktionen untersucht. Hierfür wurde eine Reaktionssequenz bestehend aus einer DeacetylierungDiazotierung-Kupplungsreaktion verwendet, um die Acetamid-Gruppe in eine Abgangsgruppe zu überführen und danach in einer MATSUDA-HECK Reaktion zu kuppeln. Mit dieser Methode konnten mehrere 1,2-Dialkenylbenzole erhalten werden und die CDG ein weiteres Mal genutzt werden. Neben der Überführung der CDG in eine Abgangsgruppe konnte diese auch in die Synthese verschiedener Heterozyklen integriert werden. Dafür erfolgte zunächst eine 1,3-Zykloaddition durch deprotonierten Tosylmethylisocanid an der elektronenarmen Sulfalkenylgruppe zur Synthese von Pyrrolen. Anschließend erfolgte eine Kupplung der PyrrolFunktion und der CDG durch Zyklokondensation, wodurch Quinoline dargestellt wurden. Durch diese Synthesen konnten Schwefelanaloga des Naturstoffes Marinoquionolin A erhalten werden.
Ein weitere übergangsmetallkatalysierte C-H-Aktivierungsreaktion, die MATSUDA-HECK Reaktion, wurde genutzt, um 1b zu mit verschieden, subtituierten Diazoniumsalzen zu arylieren. Hier konnten zahlreichen Styrenylsulfone erhalten werden. Der erfolgreiche Einsatz der Vinylsulfonylverbindungen in der Kreuzmetathese konnte innerhalb dieser Arbeit nicht erreicht werden. Daher erfolgte die Synthese verschiedener dialkenylierter Sulfonamide. Hierfür wurde die Kettenlänge der Alkenyl-Gruppe am Schwefel zwischen 2-3 und am Stickstoff zwischen 3-4 variiert. Der Einsatz der dialkenylierten Sulfonamide erfolgte in den zuvor untersuchten C-H-Aktivierungsmethoden.
N-Allyl-N-phenylethensulfonamid (3) konnte erfolgreich in der DHR und HECK Reaktion funktionalisiert werden. Hierbei erfolgte eine methodenspezifische Kupplung in Abhängigkeit von der Elektronendichte der entsprechenden Alkenyl-Gruppe. Die DHR führte zur selektiven Arylierung der Vinyl-Gruppe und die HECK Reaktion zur Arylierung an der Allyl-Gruppe. Gemischte Produkte wurden nicht erhalten. Für die weiteren Diolefine wurde komplexe Produktgemische erhalten. Des Weiteren wurden die Diolefine in der Ringschlussmetathese untersucht und die entsprechenden Sultame in sehr guten Ausbeuten erhalten. Die Verwendung der Sultame in der C-H-Aktivierung war erfolglos. Es wird vermutet, dass für diese zweifachsubstituierten Sulfonamide die vorhandenen Reaktionsbedingungen optimiert werden müssen.
Abschließend wurden verschiedene, enantiomerenreine Olefine ausgehend von Levoglucosenon dargestellt. Hierfür wurde Levoglucosenon zunächst mit einem Allyl- und 3-Butenylgrignard Reagenz umgesetzt. Die entsprechenden Produkte wurden in moderaten Ausbeuten erhalten. Eine weitere Methode begann mit der Reduktion von Levoglucosenon zum Levoglucosenol. Dieser Alkohol wurde mit Allylbromid erfolgreich verethert. Neben der Untersuchungen zur Ethersynthese, erfolgte die Veresterung von Levoglucosenol mit verschiedenen Sulfonylchloriden zu den entsprechenden Sulfonsäureestern. Diese Olefine wurden in einer Dominometathesereaktion untersucht. Ausgehend vom Allyllevoglucosenylether erfolgte die Darstellung eines Dihydrofurans.
Ökonomische Bildung digital
(2021)
On 7 February 1861, John Tyndall, professor of natural philosophy, delivered a historical lecture: he could prove that different gases absorb heat to a very different degree, which implies that the temperate conditions provided for by the Earth's atmosphere are dependent on its particular composition of gases. The theoretical foundation of climate science was laid.
Ten years later, on the other side of the Channel, a young and ambitious author was working on a comprehensive literary analysis of the French era under the Second Empire. Émile Zola had probably not heard or read of Tyndall's discovery. However, the article makes the case for reading Zola's Rougon-Macquart as an extensive story of climate change. Zola's literary attempts to capture the defining characteristic of the Second Empire led him to the insight that its various milieus were all part of the same ‘climate’: that of an all-encompassing warming. Zola suggests that this climate is man-made: the economic success of the Second Empire is based on heating, in a literal and metaphorical sense, as well as on stoking the steam-engines and creating the hypertrophic atmosphere of the hothouse that enhances life and maximises turnover and profit. In contrast to Tyndall and his audience, Zola sensed the catastrophic consequences of this warming: the Second Empire was inevitably moving towards a final débâcle, i.e. it was doomed to perish in local and ‘global’ climate catastrophes.
The article foregrounds the supplementary status of Tyndall's physical and Zola's literary knowledge. As Zola's striking intuition demonstrates, literature appears to have a privileged approach to the phenomenon of man-induced climate change.
On 7 February 1861, John Tyndall, professor of natural philosophy, delivered a historical lecture: he could prove that different gases absorb heat to a very different degree, which implies that the temperate conditions provided for by the Earth's atmosphere are dependent on its particular composition of gases. The theoretical foundation of climate science was laid.
Ten years later, on the other side of the Channel, a young and ambitious author was working on a comprehensive literary analysis of the French era under the Second Empire. Émile Zola had probably not heard or read of Tyndall's discovery. However, the article makes the case for reading Zola's Rougon-Macquart as an extensive story of climate change. Zola's literary attempts to capture the defining characteristic of the Second Empire led him to the insight that its various milieus were all part of the same ‘climate’: that of an all-encompassing warming. Zola suggests that this climate is man-made: the economic success of the Second Empire is based on heating, in a literal and metaphorical sense, as well as on stoking the steam-engines and creating the hypertrophic atmosphere of the hothouse that enhances life and maximises turnover and profit. In contrast to Tyndall and his audience, Zola sensed the catastrophic consequences of this warming: the Second Empire was inevitably moving towards a final débâcle, i.e. it was doomed to perish in local and ‘global’ climate catastrophes.
The article foregrounds the supplementary status of Tyndall's physical and Zola's literary knowledge. As Zola's striking intuition demonstrates, literature appears to have a privileged approach to the phenomenon of man-induced climate change.
§ 24 Ordnungswidrigkeiten
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§ 23 Strafbestimmung
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§§ 147-149
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§65 Kommunale Zusammenarbeit
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§ 9 Werkarten C. Musikwerke
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§ 84 Merchandisingverträge
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§ 72 Übersetzerverträge
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§ 70 Verjährung
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§ 4 Kommunalrecht
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§ 32a Clearingstelle
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§ 3 Begriffsbestimmungen
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§ 256 Nichtigkeit
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