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A series of polystyrene-block-poly(1,2-butadiene)-block-poly(2-vinyl-pyridine) (SBV) triblock terpolymers were used to prepare blends with symmetric polystyrene-block-poly(2-vinylpyridine) (SV) and poly(2-vinylpyridine)-block-poly- (cyclohexyl methacrylate) (VC) diblock copolymers. Morphological characterization was carried out by transmission electron microscopy. These triblock terpolymers self-assemble into various core-shell type or lamellar morphologies. In the SBV/SV blends, macrophase separation between the two block copolymers, continuous centrosymmetric lamellae and stacks of non-centrosymmetric lamellae with anti-parallel orientation were found. In the blends of SBV/VC, macrophase separation was never observed, what is due to the specific interactions between S and C domains. These systems showed among other morphologies also a cylindrical morphology in which rings surround the cylinders
This article describes how to use statistical data analysis to obtain models directly from data. The focus is put on finding nonlinearities within a generalized additive model. These models are found by means of backfitting or more general algorithms, like the alternating conditional expectation value one. The method is illustrated by numerically generated data. As an application, the example of vortex ripple dynamics, a highly complex fluid-granular system, is treated
Aspects of Boundary Problems in Analysis and Geometry : advances in partial differential equations
(2004)
The amphiphilic poly(ampholyte) poly(N,N-diallyl-N-hexylamine-alt-maleic acid), bearing simultaneously carboxylic acids, amines and hydrocarbon side chains, was used as a matrix to stabilize inorganic ion species (anionic as well as cationic) generated in aqueous solution from Ni(NO3)(2).6H(2)O, Co(NO3)(2).6H(2)O and (NH4)2MoO(4). Drying produces hybrid organic-inorganic blends which, due to the amphiphilicity of the copolymer, exhibit supramolecular organization in the bulk. Solid state studies show that up to two moles of metal cations (alone or together with metal anions) per repeat unit of the copolymer can be blended without loss of homogeneity in the hybrid material. A systematic screening permitted the determination of the optimal conditions for the preparation of homogeneous blends. Thermal treatment of the hybrid materials produces simple and mixed nickel and/or cobalt molybdates. The alpha- as well as the P- phase were obtained, and the mixed structures are solid solutions of simple NiMoO4 and CoMoO4