- A new method in plasma surface engineering called pulsed plasma electrolytic deposition (PPED) was applied to copper substrates. Corrosion properties of the produced layers were evaluated via potentiodynamic polarization. Results indicated relations among treatment time as well as peak applied voltage, frequency, and duty cycle on average density of TiO2 nanorods significantly. Investigation of the corrosion characteristics showed that the magnitude of corrosion resistance strongly followed from the experimental parameters of applied treatment as well as the average density of TiO2 nanorods. The average density of TiO2 nanorods measurements was done via figure analysis with minimum possible errors.