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Photochemical synthesis and properties of axially chiral naphthylpyridines
- Five alkynyl pyridines were prepared and cyclized to naphthylpyridines as the main products in the course of a Photo-Dehydro-Diels-Alder reaction. Four of the final products are axially chiral and the determination of the rotational barrier by DFT calculations, dynamic NMR and H PLC experiments is demonstrated. (C) 2011 Elsevier B.V. All rights reserved.
Author details: | Pablo WessigORCiDGND, Charlotte Pick |
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DOI: | https://doi.org/10.1016/j.jphotochem.2011.06.006 |
ISSN: | 1010-6030 |
Title of parent work (English): | Journal of photochemistry and photobiology : A, Chemistry |
Publisher: | Elsevier |
Place of publishing: | Lausanne |
Publication type: | Article |
Language: | English |
Year of first publication: | 2011 |
Publication year: | 2011 |
Release date: | 2017/03/26 |
Tag: | Axial chirality; Dynamic HPLC; Dynamic NMR; Molecular modeling; Photo-Dehydro-Diels-Alder reaction; Photochemistry |
Volume: | 222 |
Issue: | 1 |
Number of pages: | 3 |
First page: | 263 |
Last Page: | 265 |
Organizational units: | Mathematisch-Naturwissenschaftliche Fakultät / Institut für Chemie |
Peer review: | Referiert |