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The reaction of 3,4-dihydro-2H-pyran with oxalyl chloride : formation and crystal structure analysis of an unexpected bicyclic product

  • 3,4-Dihydro-2-H-pyran and oxalyl chloride react, depending on the conditions, to keto esters, a pyran-3- carboxylic acid or derivatives thereof, or to an hitherto unknown bicyclic acetal containing a vinyl chloride moiety. The structure of the latter product has been unambiguously elucidated by single-crystal X-ray structure analysis. A mechanism for its formation is proposed.

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Author details:Bernd SchmidtORCiDGND, Frank Werner, Alexandra Kelling, Uwe SchildeORCiDGND
URL:http://1960 = dx.doi.org/10.1002/jhet.456
ISSN:0022-152X
Publication type:Article
Language:English
Year of first publication:2010
Publication year:2010
Release date:2017/03/25
Source:Journal of Heterocyclic Chemistry. - ISSN 0022-152X. - 47 (2010), 5, S. 1171 - 1175
Organizational units:Mathematisch-Naturwissenschaftliche Fakultät / Institut für Chemie
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