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Temperature dependent soft x-ray absorption spectroscopy of liquids

  • A novel sample holder is introduced which allows for temperature dependent soft x-ray absorption spectroscopy of liquids in transmission mode. The setup is based on sample cells with x-ray transmissive silicon nitride windows. A cooling circuit allows for temperature regulation of the sample liquid between -10 degrees C and +50 degrees C. The setup enables to record soft x-ray absorption spectra of liquids in transmission mode with a temperature resolution of 0.5K and better. Reliability and reproducibility of the spectra are demonstrated by investigating the characteristic temperature-induced changes in the oxygen K-edge x-ray absorption spectrum of liquid water. These are compared to the corresponding changes in the oxygen K-edge spectra from x-ray Raman scattering. (C) 2014 AIP Publishing LLC.

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Metadaten
Author:Jan Meibohm, Simon Schreck, Philippe Wernet
DOI:https://doi.org/10.1063/1.4896977
ISSN:0034-6748 (print)
ISSN:1089-7623 (online)
Pubmed Id:http://www.ncbi.nlm.nih.gov/pubmed?term=25362366
Parent Title (English):Review of scientific instruments : a monthly journal devoted to scientific instruments, apparatus, and techniques
Publisher:American Institute of Physics
Place of publication:Melville
Document Type:Article
Language:English
Year of first Publication:2014
Year of Completion:2014
Release Date:2017/03/27
Volume:85
Issue:10
Pagenumber:7
Organizational units:Mathematisch-Naturwissenschaftliche Fakultät / Institut für Physik und Astronomie
Peer Review:Referiert