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2,2 '-Biphenols via protecting group-free thermal or microwave-accelerated suzuki-miyaura coupling in water

  • User-friendly protocols for the protecting group-free synthesis of 2,2'-biphenols via Suzuki-Miyaura coupling of o-halophenols and o-boronophenol are presented. The reactions proceed in water in the presence of simple additives such as K2CO3, KOH, KF, or TBAF and with commercially available Pd/C as precatalyst. Expensive or laboriously synthesized ligands or other additives are not required. In the case of bromophenols, efficient rate acceleration and short reaction times were accomplished by microwave irradiation.

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Metadaten
Author details:Bernd SchmidtORCiDGND, Martin Riemer, Manfred KarrasORCiDGND
DOI:https://doi.org/10.1021/jo401398n
ISSN:0022-3263
Title of parent work (English):The journal of organic chemistry
Publisher:American Chemical Society
Place of publishing:Washington
Publication type:Article
Language:English
Year of first publication:2013
Publication year:2013
Release date:2017/03/26
Volume:78
Issue:17
Number of pages:9
First page:8680
Last Page:8688
Organizational units:Mathematisch-Naturwissenschaftliche Fakultät / Institut für Chemie
Peer review:Referiert
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