TY - JOUR A1 - Mihoc, Carmen A1 - Schick, Daniel A1 - Lütgens, Matthias A1 - Lathe, Christian A1 - Burkel, Eberhard T1 - Formation of Al67Cu23Fe10 quasicrystals by microwave heating JF - International journal of materials research : Zeitschrift für Metallkunde N2 - The present work was carried out to compare the formation of single icosahedral phase during conventional heating and microwave processing. Al67Cu23Fe10 alloy powder was synthesized from high purity (99.9%) powder elements by mechanical alloying. Differential scanning calorimetry combined with in-situ synchrotron energy dispersive X-ray diffraction was used to identify the main solid state reactions and the phase evolution of the powders. Inductive microwave processing in the magnetic field anti-node was performed to obtain the quasicrystalline phase in only a few seconds. Due to the rapid cooling of the sample it was possible to stabilize the icosahedral phase against its competing quasicrystalline approximants. Laboratory X-ray diffraction analysis was used to characterise the atomic structure of the specimen and scanning electron microscopy was used to characterise the microstructure after the microwave processing. KW - Quasicrystals KW - Microwave processing KW - Mechanical alloying Y1 - 2012 U6 - https://doi.org/10.3139/146.110786 SN - 1862-5282 VL - 103 IS - 11 SP - 1340 EP - 1344 PB - Hanser CY - München ER -