TY  - JOUR
A1  - Grunwald, Nicolas
A1  - Kelling, Alexandra
A1  - Holdt, Hans-Jürgen
A1  - Schilde, Uwe
T1  - The crystal structure of 1,1′-bisisoquinoline, C18H12N2
JF  - Zeitschrift für Kristallographie : international journal for structural, physical and chemical aspects of crystalline materials. New crystal structures
N2  - C18H12N2, tetragonal, I41/a (no. 88), a=13.8885(6) Å,
c=13.6718(6) Å, V =2637.2(3) Å3, Z =8, Rgt(F)=0.0295,
wRref(F2)=0.0854, T =210 K.
CCDC no.: 631823
Y1  - 2017
U6  - https://doi.org/10.1515/ncrs-2017-0088
VL  - 232
IS  - 5
SP  - 839
EP  - 841
PB  - de Gruyter
CY  - Berlin
ER  - 
TY  - JOUR
A1  - Grunwald, Nicolas
A1  - Kelling, Alexandra
A1  - Holdt, Hans-Jürgen
A1  - Schilde, Uwe
T1  - The crystal structure of 1,1′-bisisoquinoline, C18H12N2
JF  - Zeitschrift für Kristallographie : international journal for structural, physical and chemical aspects of crystalline materials ; New crystal structures
N2  - C18H12N2, tetragonal, I4(1)/a (no. 88), a = 13.8885(6) angstrom, c = 13.6718(6) angstrom, V = 2637.2(3) angstrom(3), Z = 8, R-gt(F) = 0.0295, wR(ref)(F-2) = 0.0854, T = 210 K.
Y1  - 2017
U6  - https://doi.org/10.1515/ncrs-2017-0088
SN  - 1433-7266
VL  - 232
SP  - 839
EP  - 841
PB  - De Gruyter
CY  - Berlin
ER  - 
TY  - JOUR
A1  - Kammer, Stefan
A1  - Müller, Holger
A1  - Grunwald, Nicolas
A1  - Bellin, Anja
A1  - Kelling, Alexandra
A1  - Schilde, Uwe
A1  - Mickler, Wulfhard
A1  - Dosche, Carsten
A1  - Holdt, Hans-Jürgen
T1  - Supramolecular assemblies with honeycomb structures by pi-pi stacking of octahedral metal complexes of 1,12- diazaperylene
N2  - Homoleptic Ni-II and Fe-II complexes of the "large-surface" phenanthroline-type ligand 1,12-diazaperylene (dap), [Ni(dap)(3)](BF4)(2) (1) and [Fe(dap)(3)](PF6)(2) (2), respectively, were synthesized. In the crystal structure the complex cation [M(dap)(3)](2+) (M = Ni, Fe) exhibits C-3 symmetry and interacts with three other cations by pi-pi stacking. It forms a new metalla-supramolecular assembly with a honeycomb structure containing nanochannels running parallel to the crystallographic c axis. Aggregation by pi-pi stacking between metal complexes of "large-surface" ligands should give new perspectives for inorganic supramolecular chemistry.
Y1  - 2006
UR  - http://www3.interscience.wiley.com/cgi-bin/jhome/27721/
U6  - https://doi.org/10.1002/ejic.200600092
SN  - 1343-1948
ER  - 
TY  - JOUR
A1  - Starke, Ines
A1  - Kammer, Stefan
A1  - Grunwald, Nicolas
A1  - Schilde, Uwe
A1  - Holdt, Hans-Jürgen
A1  - Kleinpeter, Erich
T1  - Complexation of diazaperylene and bisisoquinoline with transition metal ions in the gas phase studied by electrospray ionization mass spectrometry
N2  - The complex formation of the ligands 1,12-diazaperylene (dap), 1,1-bisisoquinoline (bis), 2,2-bipyridine (bpy) and 1,10-phenanthroline (phen) with transition metal ions (M = Fe, Co, Ni, Cu, Zn, Ru, Os, Re, Pd, Pt, Ag and Cd) in the gas phase has been studied by electrospray ionization mass spectrometry. With the exception of Ru, Os, Fe, Ni and Cu, singly charged complexes [MLn]+ (n = 1,2) were observed. The complexes of dap and bis with Ru, Os, Fe and Ni ions, and the mixed ligand complexes with bpy and phen, are preferably of the doubly charged type [ML3]2+. In addition, collision- induced dissociation (CID) measurements were employed to evaluate the relative stabilities of these complexes. The CID experiments of mixed-ligand complexes which contain both dap and phen or dap and bpy exhibit preferential elimination of bpy, indicating that bpy is a weaker ligand than phen and dap.
Y1  - 2008
ER  -