@article{CabezaMishurovaGarcesetal.2017, author = {Cabeza, Sandra and Mishurova, Tatiana and Garc{\´e}s, Gonzales and Sevostianov, Igor and Requena, Guillermo and Bruno, Giovanni}, title = {Stress-induced damage evolution in cast AlSi12CuMgNi alloy with one- and two-ceramic reinforcements}, series = {Journal of materials science}, volume = {52}, journal = {Journal of materials science}, publisher = {Springer}, address = {New York}, issn = {0022-2461}, doi = {10.1007/s10853-017-1182-7}, pages = {10198 -- 10216}, year = {2017}, abstract = {Two composites, consisting of an as-cast AlSi12CuMgNi alloy reinforced with 15 vol\% Al2O3 short fibres and with 7 vol\% Al2O3 short fibres + 15 vol\% SiC particles, were studied. Synchrotron computed tomography disclosed distribution, orientation, and volume fraction of the different phases. In-situ compression tests during neutron diffraction in direction parallel to the fibres plane revealed the load partition between phases. Internal damage (fragmentation) of the Si phase and Al2O3 fibres was directly observed in CT reconstructions. Significant debonding between Al matrix and SiC particles was also found. Finally, based on the Maxwell scheme, a micromechanical model was utilized for the new composite with two-ceramic reinforcements; it rationalizes the experimental data and predicts the evolution of all internal stress components in each phase.}, language = {en} } @article{EvsevleevMishurovaCabezaetal.2018, author = {Evsevleev, Sergei and Mishurova, Tatiana and Cabeza, Sandra and Koos, R. and Sevostianov, Igor and Garc{\´e}s, Gonzales and Requena, Guillermo and Fernandez, R. and Bruno, Giovanni}, title = {The role of intermetallics in stress partitioning and damage evolution of AlSil2CuMgNi alloy}, series = {Materials Science and Engineering: A-Structural materials: properties, microstructure and processing}, volume = {736}, journal = {Materials Science and Engineering: A-Structural materials: properties, microstructure and processing}, publisher = {Elsevier}, address = {Lausanne}, issn = {0921-5093}, doi = {10.1016/j.msea.2018.08.070}, pages = {453 -- 464}, year = {2018}, abstract = {Load partitioning between phases in a cast AlSi12CuMgNi alloy was investigated by in-situ compression test during neutron diffraction experiments. Computed tomography (CT) was used to determine volume fractions of eutectic Si and intermetallic (IM) phases, and to assess internal damage after ex-situ compression tests. The CT reconstructed volumes showed the interconnectivity of IM phases, which build a 3D network together with eutectic Si. Large stresses were found in IMs, revealing their significant role as a reinforcement for the alloy. An existing micromechanical model based on Maxwell scheme was extended to the present case, assuming the alloy as a three-phase composite (Al matrix, eutectic Si, IM phases). The model agrees well with the experimental data. Moreover, it allows predicting the principal stresses in each phase, while experiments can only determine stress differences between the axial and radial sample directions. Finally, we showed that the addition of alloying elements not only allowed developing a 3D interconnected network, but also improved the strength of the Al matrix, and the ability of the alloy constituents to bear mechanical load.}, language = {en} } @article{FernandezCabezaMishurovaetal.2018, author = {Fernandez, R. and Cabeza, Sandra and Mishurova, Tatiana and Fernandez-Castrillo, P. and Gonzalez-Doncel, Gaspar and Bruno, Giovanni}, title = {Residual stress and yield strength evolution with annealing treatments in an age-hardenable aluminum alloy matrix composite}, series = {Materials Science and Engineering: A}, volume = {731}, journal = {Materials Science and Engineering: A}, publisher = {Elsevier}, address = {Lausanne}, issn = {0921-5093}, doi = {10.1016/j.msea.2018.06.031}, pages = {344 -- 350}, year = {2018}, abstract = {We investigated the possibility of minimizing tensile matrix residual stresses in age hardenable aluminum alloy metal matrix composites without detrimentally affect their mechanical properties (such as yield strength). Specifically, we performed thermal treatments at different temperatures and times in an age-hardenable aluminum matrix composite 2014Al-15vol\%Al2O3. Using X-ray synchrotron radiation diffraction and mechanical tests, we show that below a certain treatment temperature (250 degrees C) it is possible to identify an appropriate thermal treatment capable of relaxing residual stress in this composite while even increasing its yield strength, with respect to the as processed conditions.}, language = {en} } @article{MishurovaArtztHaubrichetal.2018, author = {Mishurova, Tatiana and Artzt, Katia and Haubrich, Jan and Requena, Guillermo and Bruno, Giovanni}, title = {New aspects about the search for the most relevant parameters optimizing SLM materials}, series = {Additive manufacturing}, volume = {25}, journal = {Additive manufacturing}, publisher = {Elsevier}, address = {Amsterdam}, issn = {2214-8604}, doi = {10.1016/j.addma.2018.11.023}, pages = {325 -- 334}, year = {2018}, abstract = {While the volumetric energy density is commonly used to qualify a process parameter set, and to quantify its influence on the microstructure and performance of additively manufactured (AM) materials and components, it has been already shown that this description is by no means exhaustive. In this work, new aspects of the optimization of the selective laser melting process are investigated for AM Ti-6Al-4V. We focus on the amount of near-surface residual stress (RS), often blamed for the failure of components, and on the porosity characteristics (amount and spatial distribution). First, using synchrotron x-ray diffraction we show that higher RS in the subsurface region is generated if a lower energy density is used. Second, we show that laser de-focusing and sample positioning inside the build chamber also play an eminent role, and we quantify this influence. In parallel, using X-ray Computed Tomography, we observe that porosity is mainly concentrated in the contour region, except in the case where the laser speed is small. The low values of porosity (less than 1\%) do not influence RS.}, language = {en} } @article{MishurovaArtztHaubrichetal.2019, author = {Mishurova, Tatiana and Artzt, Katia and Haubrich, Jan and Requena, Guillermo and Bruno, Giovanni}, title = {Exploring the correlation between subsurface residual stresses and manufacturing parameters in laser powder bed fused Ti-6Al-4V}, series = {Metals}, volume = {9}, journal = {Metals}, number = {2}, publisher = {MDPI}, address = {Basel}, issn = {2075-4701}, doi = {10.3390/met9020261}, pages = {13}, year = {2019}, abstract = {Subsurface residual stresses (RS) were investigated in Ti-6Al-4V cuboid samples by means of X-ray synchrotron diffraction. The samples were manufactured by laser powder bed fusion (LPBF) applying different processing parameters, not commonly considered in open literature, in order to assess their influence on RS state. While investigating the effect of process parameters used for the calculation of volumetric energy density (such as laser velocity, laser power and hatch distance), we observed that an increase of energy density led to a decrease of RS, although not to the same extent for every parameter variation. Additionally, the effect of support structure, sample roughness and LPBF machine effects potentially coming from Ar flow were studied. We observed no influence of support structure on subsurface RS while the orientation with respect to Ar flow showed to have an impact on RS. We conclude recommending monitoring such parameters to improve part reliability and reproducibility.}, language = {en} } @article{MishurovaBrunoEvsevleevetal.2020, author = {Mishurova, Tatiana and Bruno, Giovanni and Evsevleev, Sergei and Sevostianov, Igor}, title = {Determination of macroscopic stress from diffraction experiments}, series = {Journal of applied physics}, volume = {128}, journal = {Journal of applied physics}, number = {2}, publisher = {American Institute of Physics}, address = {Melville}, issn = {0021-8979}, doi = {10.1063/5.0009101}, pages = {14}, year = {2020}, abstract = {The paper is motivated by some inconsistencies and contradictions present in the literature on the calculation of the so-called diffraction elastic constants. In an attempt at unifying the views that the two communities of Materials Science and Mechanics of Materials have on the subject, we revisit and define the terminology used in the field. We also clarify the limitations of the commonly used approaches and show that a unified methodology is also applicable to textured materials with a nearly arbitrary grain shape. We finally compare the predictions based on this methodology with experimental data obtained by in situ synchrotron radiation diffraction on additively manufactured Ti-6Al-4V alloy. We show that (a) the transverse isotropy of the material yields good agreement between the best-fit isotropy approximation (equivalent to the classic Kroner's model) and the experimental data and (b) the use of a general framework allows the calculation of all components of the tensor of diffraction elastic constants, which are not easily measurable by diffraction methods. This allows us to extend the current state-of-the-art with a predictive tool.}, language = {en} } @article{MishurovaCabezaArtztetal.2017, author = {Mishurova, Tatiana and Cabeza, Sandra and Artzt, Katia and Haubrich, Jan and Klaus, Manuela and Genzel, Christoph and Requena, Guillermo and Bruno, Giovanni}, title = {An Assessment of Subsurface Residual Stress Analysis in SLM Ti-6Al-4V}, series = {Materials}, volume = {10}, journal = {Materials}, publisher = {MDPI}, address = {Basel}, issn = {1996-1944}, doi = {10.3390/ma10040348}, pages = {14}, year = {2017}, abstract = {Ti-6Al-4V bridges were additively fabricated by selective laser melting (SLM) under different scanning speed conditions, to compare the effect of process energy density on the residual stress state. Subsurface lattice strain characterization was conducted by means of synchrotron diffraction in energy dispersive mode. High tensile strain gradients were found at the frontal surface for samples in an as-built condition. The geometry of the samples promotes increasing strains towards the pillar of the bridges. We observed that the higher the laser energy density during fabrication, the lower the lattice strains. A relief of lattice strains takes place after heat treatment.}, language = {en} } @article{MishurovaCabezaThiedeetal.2018, author = {Mishurova, Tatiana and Cabeza, Sandra and Thiede, Tobias and Nadammal, Naresh and Kromm, Arne and Klaus, Manuela and Genzel, Christoph and Haberland, Christoph and Bruno, Giovanni}, title = {The Influence of the Support Structure on Residual Stress and Distortion in SLM Inconel 718 Parts}, series = {Metallurgical and Materials Transactions A}, volume = {49A}, journal = {Metallurgical and Materials Transactions A}, number = {7}, publisher = {Springer}, address = {New York}, issn = {1073-5623}, doi = {10.1007/s11661-018-4653-9}, pages = {3038 -- 3046}, year = {2018}, abstract = {The effect of support structure and of removal from the base plate on the residual stress state in selective laser melted IN718 parts was studied by means of synchrotron X-ray diffraction. The residual stresses in subsurface region of two elongated prisms in as-built condition and after removal from the base plate were determined. One sample was directly built on a base plate and another one on a support structure. Also, the distortion on the top surface due to stress release was measured by contact profilometry. High tensile residual stress values were found, with pronounced stress gradient along the hatching direction. In the sample on support, stress redistribution took place after removal from the base plate, as opposed to simple stress relaxation for the sample without support. The sample on support structure showed larger distortion compared to sample without support. We conclude that the use of a support decreases stress values but stress-relieving heat treatments are still needed.}, language = {en} } @article{MishurovaStegemannLyamkinetal.2022, author = {Mishurova, Tatiana and Stegemann, Robert and Lyamkin, Viktor and Cabeza, Sandra and Evsevleev, Sergei and Pelkner, Matthias and Bruno, Giovanni}, title = {Subsurface and bulk residual stress analysis of S235JRC+C Steel TIG weld by diffraction and magnetic stray field measurements}, series = {Experimental mechanics : an international journal of the Society for Experimental Mechanics}, volume = {62}, journal = {Experimental mechanics : an international journal of the Society for Experimental Mechanics}, number = {6}, publisher = {Springer}, address = {New York}, issn = {0014-4851}, doi = {10.1007/s11340-022-00841-x}, pages = {1017 -- 1025}, year = {2022}, abstract = {Background Due to physical coupling between mechanical stress and magnetization in ferromagnetic materials, it is assumed in the literature that the distribution of the magnetic stray field corresponds to the internal (residual) stress of the specimen. The correlation is, however, not trivial, since the magnetic stray field is also influenced by the microstructure and the geometry of component. The understanding of the correlation between residual stress and magnetic stray field could help to evaluate the integrity of welded components. Objective This study aims at understanding the possible correlation of subsurface and bulk residual stress with magnetic stray field in a low carbon steel weld. Methods The residual stress was determined by synchrotron X-ray diffraction (SXRD, subsurface region) and by neutron diffraction (ND, bulk region). SXRD possesses a higher spatial resolution than ND. Magnetic stray fields were mapped by utilizing high-spatial-resolution giant magneto resistance (GMR) sensors. Results The subsurface residual stress overall correlates better with the magnetic stray field distribution than the bulk stress. This correlation is especially visible in the regions outside the heat affected zone, where the influence of the microstructural features is less pronounced but steep residual stress gradients are present. Conclusions It was demonstrated that the localized stray field sources without any obvious microstructural variations are associated with steep stress gradients. The good correlation between subsurface residual stress and magnetic signal indicates that the source of the magnetic stray fields is to be found in the range of the penetration depth of the SXRD measurements.}, language = {en} } @article{MishurovaSydowThiedeetal.2020, author = {Mishurova, Tatiana and Sydow, Benjamin and Thiede, Tobias and Sizova, Irina and Ulbricht, Alexander and Bambach, Markus and Bruno, Giovanni}, title = {Residual stress and microstructure of a Ti-6Al-4V Wire Arc Additive Manufacturing hybrid demonstrator}, series = {Metals}, volume = {10}, journal = {Metals}, number = {6}, publisher = {MDPI}, address = {Basel}, issn = {2075-4701}, doi = {10.3390/met10060701}, pages = {15}, year = {2020}, abstract = {Wire Arc Additive Manufacturing (WAAM) features high deposition rates and, thus, allows production of large components that are relevant for aerospace applications. However, a lot of aerospace parts are currently produced by forging or machining alone to ensure fast production and to obtain good mechanical properties; the use of these conventional process routes causes high tooling and material costs. A hybrid approach (a combination of forging and WAAM) allows making production more efficient. In this fashion, further structural or functional features can be built in any direction without using additional tools for every part. By using a combination of forging basic geometries with one tool set and adding the functional features by means of WAAM, the tool costs and material waste can be reduced compared to either completely forged or machined parts. One of the factors influencing the structural integrity of additively manufactured parts are (high) residual stresses, generated during the build process. In this study, the triaxial residual stress profiles in a hybrid WAAM part are reported, as determined by neutron diffraction. The analysis is complemented by microstructural investigations, showing a gradient of microstructure (shape and size of grains) along the part height. The highest residual stresses were found in the transition zone (between WAAM and forged part). The total stress range showed to be lower than expected for WAAM components. This could be explained by the thermal history of the component.}, language = {en} }